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171Yb cross-polarization magic angle spinning NMR spectroscopic studies of organometallic compounds:? bis(cyclopentadienyl) derivatives
journal contribution
posted on 2023-06-07, 23:02 authored by Julian M Keates, Gerard A LawlessA series of nine Yb(II) bis(cyclopentadienyl) complexes have been studied by 171Yb CP MAS (cross polarization magic angle spinning) NMR spectroscopy. The optimization of the cross polarization conditions are described. The proton T1? values have been determined. The spinning side band manifold for each compound has been analyzed. The derived chemical shift tensor data are discussed with respect to molecular structure elucidation.
History
Publication status
- Published
Journal
OrganometallicsPublisher
American Chemical SocietyExternal DOI
Issue
13Volume
16Page range
2842 - 2846ISBN
0276-7333Department affiliated with
- Chemistry Publications
Full text available
- No
Peer reviewed?
- Yes