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Microwave-mediated synthesis of N-methyliminodiacetic acid (MIDA) boronates
journal contributionposted on 2023-06-08, 20:40 authored by Adam J Close, Paul Kemmitt, Matthew K Emmerson, John SpencerJohn Spencer
A library of over 20, mainly aryl or heteroaryl, N-methyliminodiacetic acid (MIDA) boronates have been synthesised. A rapid microwave-mediated (MW) method (5–10 min) has been developed using polyethylene glycol 300 (PEG 300) as solvent. However, acetonitrile (MeCN) and dimethylformamide (DMF) were found to be alternative solvents, the latter especially for 2-substituted aryl boronic acids.
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